Effect of Nanoclay Loading on the Hardness Property of Epoxy Composites
1 Department of Chemical Engineering, Nasarawa State University Keffi, Nigeria
2 Department of Polymer and Textile Engineering, Ahmadu Bello University, Zaria, Nigeria
3 Department of polymer and Textile Engineering, Ahmadu Bello University, Zaria,
* Corresponding author: egerebisike@nuk.edu.ng
2 Department of Polymer and Textile Engineering, Ahmadu Bello University, Zaria, Nigeria
3 Department of polymer and Textile Engineering, Ahmadu Bello University, Zaria,
* Corresponding author: egerebisike@nuk.edu.ng
Abstract
This study examines the influence of nanoclay loading on the hardness properties of epoxy composites. Nanocomposites
were fabricated using varying weight percentages of nanoclay and epoxy via the hand layup method with an open mould.
Mechanical characterisation was carried out using a Rockwell hardness tester, while the dispersion and morphology of
nanoclay particles within the epoxy matrix were analysed using Scanning Electron Microscopy (SEM). The composite
containing 4 wt.% nanoclay (nanoclay-to-epoxy ratio of 4:96) exhibited the highest hardness value of 109.60 HRA,
representing a 65% improvement over the control sample (neat epoxy). The results demonstrate that the incorporation
of nanoclay significantly enhances the hardness of epoxy, with hardness values increasing proportionally with nanoclay
content up to an optimum level. Beyond this saturation point, a decline in hardness was observed, attributed to particle
agglomeration and poor interfacial adhesion between the nanoclay and the epoxy matrix. Overall, the findings establish
nanoclay as an effective reinforcement material for epoxy polymers where improved hardness is required.
Keywords
Nanotechnology
Nanocomposite
Epoxy
Nanoclay
Hardness and SEM
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How to Cite
B.C, E., L.O, Y., & Abdulrahman, A. S. (2024). Effect of Nanoclay Loading on the Hardness Property of Epoxy Composites. Nigerian Journal of Materials Science and Engineering, 14(1), 48-53.
E. B.C, Y. L.O, and A. S. Abdulrahman, "Effect of Nanoclay Loading on the Hardness Property of Epoxy Composites," Nigerian Journal of Materials Science and Engineering, vol. 14, no. 1, pp. 48-53, June 2024.